{"id":364073,"date":"2024-10-20T01:48:54","date_gmt":"2024-10-20T01:48:54","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-15199-12020\/"},"modified":"2024-10-26T02:51:54","modified_gmt":"2024-10-26T02:51:54","slug":"bs-en-15199-12020","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-15199-12020\/","title":{"rendered":"BS EN 15199-1:2020"},"content":{"rendered":"

This document specifies a method for the determination of the boiling range distribution of petroleum products by capillary gas chromatography using flame ionization detection. The standard is applicable to materials having a vapour pressure low enough to permit sampling at ambient temperature and a boiling range of at least 100 \u00b0C. The standard is applicable to distillates with initial boiling points (IBP) above 100 \u00b0C and final boiling points (FBP) below 750 \u00b0C, for example, middle distillates and lubricating base stocks.<\/p>\n

The test method is not applicable for the analysis of petroleum or petroleum products containing low molecular weight components (for example naphtha\u2019s, reformates, gasolines) or middle distillates like Diesel and Jet fuel.<\/p>\n

Petroleum or petroleum products containing blending components which contain heteroatoms (for example alcohols, ethers, acids, or esters) or residue are not to be analysed by this test method.<\/p>\n

\n
\n NOTE\n <\/div>\n

For the purposes of this document, the terms \u201c% ( m<\/i>\/ m<\/i>)\u201d and \u201c% ( V<\/i>\/ V<\/i>)\u201d are used to represent respectively the mass fraction and the volume fraction.<\/p>\n<\/div>\n

\n
\n WARNING\n <\/div>\n

The use of this document can involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.<\/p>\n<\/div>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
2<\/td>\nundefined <\/td>\n<\/tr>\n
6<\/td>\n1 Scope
2 Normative references
3 Terms and definitions <\/td>\n<\/tr>\n
8<\/td>\n4 Principle
5 Reagents and materials <\/td>\n<\/tr>\n
11<\/td>\n6 Apparatus <\/td>\n<\/tr>\n
13<\/td>\n7 Sampling
8 Preparation of the apparatus
8.1 Gas chromatograph preparation
8.2 System performance check
9 Sample preparation
10 Calibration <\/td>\n<\/tr>\n
15<\/td>\n11 Procedure <\/td>\n<\/tr>\n
16<\/td>\n12 Visual inspection of the chromatograms
13 Calculation
14 Expression of results
15 Precision
15.1 General <\/td>\n<\/tr>\n
17<\/td>\n15.2 Repeatability
15.3 Reproducibility <\/td>\n<\/tr>\n
18<\/td>\n16 Test report <\/td>\n<\/tr>\n
19<\/td>\nAnnex A (normative)Calculation procedure
A.1 Starting conditions
A.1.1 Sample data array, N area slices
A.1.2 Blank data array, N area slices
A.1.3 Retention times of n-paraffins
A.1.4 Boiling points of n-paraffins
A.1.5 Solvent exclusion time
A.2 Subtraction of the blank from the sample <\/td>\n<\/tr>\n
20<\/td>\nA.3 Zero data slices
A.4 Total chromatogram area
A.5 Start of sample elution time <\/td>\n<\/tr>\n
21<\/td>\nA.6 End of sample elution time
A.7 Total corrected sample area
A.8 Normalization to area percentage
A.9 Retention time corresponding to percent off
A.9.1 Initial boiling point
A.9.2 Intermediate boiling points <\/td>\n<\/tr>\n
22<\/td>\nA.9.3 Final boiling point
A.9.4 Overall procedure
A.10 Conversion of retention times to boiling points <\/td>\n<\/tr>\n
24<\/td>\nAnnex B (normative)System performance check
B.1 Frequency
B.2 Column resolution
B.3 Detector response (gravimetric blend) <\/td>\n<\/tr>\n
25<\/td>\nB.4 Skewing of peak <\/td>\n<\/tr>\n
26<\/td>\nAnnex C (normative)Boiling points of n-alkanes <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

Petroleum products. Determination of boiling range distribution by gas chromatography method – Middle distillates and lubricating base oils<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
BSI<\/b><\/a><\/td>\n2021<\/td>\n30<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":364082,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-364073","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/364073","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/364082"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=364073"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=364073"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=364073"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}