{"id":291484,"date":"2024-10-19T19:47:30","date_gmt":"2024-10-19T19:47:30","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bsi-pd-iso-ts-251382019-tc\/"},"modified":"2024-10-25T16:49:52","modified_gmt":"2024-10-25T16:49:52","slug":"bsi-pd-iso-ts-251382019-tc","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bsi-pd-iso-ts-251382019-tc\/","title":{"rendered":"BSI PD ISO\/TS 25138:2019 – TC"},"content":{"rendered":"

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
52<\/td>\nundefined <\/td>\n<\/tr>\n
57<\/td>\nForeword <\/td>\n<\/tr>\n
59<\/td>\n1 Scope
2 Normative references
3 Terms and definitions <\/td>\n<\/tr>\n
60<\/td>\n4 Principle
5 Apparatus
5.1 Glow-discharge optical-emission spectrometer
5.1.1 General
5.1.2 Selection of spectral lines <\/td>\n<\/tr>\n
61<\/td>\n5.1.3 Selection of glow-discharge source type <\/td>\n<\/tr>\n
62<\/td>\n6 Adjusting the glow-discharge spectrometer system settings
6.1 General
6.2 Setting the parameters of a DC source
6.2.1 Constant applied current and voltage <\/td>\n<\/tr>\n
63<\/td>\n6.2.2 Constant applied current and pressure <\/td>\n<\/tr>\n
64<\/td>\n6.2.3 Constant voltage and pressure
6.3 Setting the discharge parameters of an RF source
6.3.1 General
6.3.2 Constant applied voltage and pressure <\/td>\n<\/tr>\n
65<\/td>\n6.3.3 Constant applied power and DC bias voltage
6.3.4 Constant effective power and RF voltage
6.4 Minimum performance requirements
6.4.1 General <\/td>\n<\/tr>\n
66<\/td>\n6.4.2 Minimum repeatability
6.4.3 Detection limit <\/td>\n<\/tr>\n
67<\/td>\n7 Sampling <\/td>\n<\/tr>\n
68<\/td>\n8 Calibration
8.1 General
8.2 Calibration samples
8.2.1 General
8.2.2 Low alloy iron or steel samples <\/td>\n<\/tr>\n
69<\/td>\n8.2.3 Stainless-steel samples
8.2.4 Nickel alloy samples
8.2.5 Copper alloy samples
8.2.6 Titanium alloy samples
8.2.7 Silicon samples
8.2.8 Aluminium alloy samples
8.2.9 High-oxygen samples
8.2.10 High-carbon samples
8.2.11 High-nitrogen samples
8.2.12 High-hydrogen samples
8.2.13 High-purity copper samples <\/td>\n<\/tr>\n
70<\/td>\n8.3 Validation samples
8.3.1 General
8.3.2 Hot-rolled low-alloy steel
8.3.3 Oxidized silicon wafers
8.3.4 TiN-coated samples
8.3.5 Anodized Al2O3 samples
8.3.6 TiO2-coated samples
8.4 Determination of the sputtering rate of calibration and validation samples <\/td>\n<\/tr>\n
72<\/td>\n8.5 Emission intensity measurements of calibration samples
8.6 Calculation of calibration formulae
8.7 Validation of the calibration
8.7.1 General <\/td>\n<\/tr>\n
73<\/td>\n8.7.2 Checking analytical accuracy using bulk reference materials
8.7.3 Checking analytical accuracy using metal oxide reference materials
8.8 Verification and drift correction <\/td>\n<\/tr>\n
74<\/td>\n9 Analysis of test samples
9.1 Adjusting discharge parameters
9.2 Setting of measuring time and data acquisition rate
9.3 Quantifying depth profiles of test samples <\/td>\n<\/tr>\n
75<\/td>\n10 Expression of results
10.1 Expression of quantitative depth profile
10.2 Determination of metal oxide mass per unit area <\/td>\n<\/tr>\n
76<\/td>\n10.3 Determination of the average mass fractions of the elements in the oxide
11 Precision <\/td>\n<\/tr>\n
77<\/td>\n12 Test report <\/td>\n<\/tr>\n
78<\/td>\nAnnex A (informative) Calculation of calibration constants and quantitative evaluation ofdepth profiles <\/td>\n<\/tr>\n
90<\/td>\nAnnex B (informative) Suggested spectral lines for determination of given elements <\/td>\n<\/tr>\n
92<\/td>\nAnnex C (informative) Examples of oxide density and the corresponding quantity \u03c1O <\/td>\n<\/tr>\n
93<\/td>\nAnnex D (informative) Report on interlaboratory testing of metal oxide films <\/td>\n<\/tr>\n
98<\/td>\nBibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

Tracked Changes. Surface chemical analysis. Analysis of metal oxide films by glow-discharge optical-emission spectrometry<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
BSI<\/b><\/a><\/td>\n2020<\/td>\n100<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":291491,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[1000,2641],"product_tag":[],"class_list":{"0":"post-291484","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-71-040-40","7":"product_cat-bsi","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/291484","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/291491"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=291484"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=291484"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=291484"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}