{"id":338619,"date":"2024-10-19T23:41:53","date_gmt":"2024-10-19T23:41:53","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-iso-22634-12019\/"},"modified":"2024-10-25T22:48:10","modified_gmt":"2024-10-25T22:48:10","slug":"bs-iso-22634-12019","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-iso-22634-12019\/","title":{"rendered":"BS ISO 22634-1:2019"},"content":{"rendered":"
This document specifies a method for the determination of benzo[a]pyrene (B[a]P) in the total particulate matter (TPM) of cigarette mainstream smoke using gas chromatography\/mass spectrometry (GC\/MS) with methanol as extraction solvent.<\/p>\n
This method is specified using ISO 3308<\/span><\/span> smoking parameters. An alternative method for the determination of B[a]P is specified in ISO 22634-2<\/span><\/span> with a different clean-up using cyclohexane solvent and a shorter total analytical time.<\/p>\n Cigarettes. Determination of benzo[a]pyrene in cigarette mainstream smoke using GC\/MS – Method using methanol as extraction solvent<\/b><\/p>\nPDF Catalog<\/h4>\n
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\n PDF Pages<\/th>\n PDF Title<\/th>\n<\/tr>\n \n 2<\/td>\n National foreword <\/td>\n<\/tr>\n \n 6<\/td>\n Foreword <\/td>\n<\/tr>\n \n 7<\/td>\n Introduction <\/td>\n<\/tr>\n \n 9<\/td>\n 1 Scope
2 Normative references
3 Terms and definitions
4 Principle <\/td>\n<\/tr>\n\n 10<\/td>\n 5 Apparatus
6 Reagents <\/td>\n<\/tr>\n\n 11<\/td>\n 7 Standards
7.1 General
7.2 Primary B[a]P stock solution
7.3 Secondary B[a]P stock solution
7.4 B[a]P-d12 stock solution
7.5 B[a]P-d12 spiking solution
7.6 Working standard solutions
7.7 Storage of standard solutions <\/td>\n<\/tr>\n\n 12<\/td>\n 8 Preparation of sample
8.1 Sampling
8.2 Smoking
8.3 Glass-fibre filter pad extraction
8.4 Sample clean-up <\/td>\n<\/tr>\n\n 13<\/td>\n 9 Determination
9.1 GC\/MS operating conditions <\/td>\n<\/tr>\n\n 14<\/td>\n 9.2 Calibration
9.3 Determination of B[a]P
9.4 Calculation
10 Repeatability and reproducibility <\/td>\n<\/tr>\n\n 15<\/td>\n 11 Test report
11.1 General
11.2 Characteristic data about the cigarette
11.3 Data about sampling <\/td>\n<\/tr>\n\n 16<\/td>\n 11.4 Description of the test
11.5 Test results <\/td>\n<\/tr>\n\n 17<\/td>\n Annex A (informative) Example of a chromatogram of a cigarette smoke extract <\/td>\n<\/tr>\n \n 19<\/td>\n Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" \n\n
\n Published By<\/td>\n Publication Date<\/td>\n Number of Pages<\/td>\n<\/tr>\n \n BSI<\/b><\/a><\/td>\n 2019<\/td>\n 20<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":338626,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-338619","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/338619","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/338626"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=338619"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=338619"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=338619"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}