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BSI PD IEC/TS 62607-6-4:2016

$102.76

Nanomanufacturing. Key control characteristics – Graphene. Surface conductance measurement using resonant cavity

Published By Publication Date Number of Pages
BSI 2016 22
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This part of IEC 62607 establishes a method for determining the surface conductance of two-dimensional (2D) single-layer or multi-layer atomically thin nano-carbon graphene structures. These are synthesized by chemical vapour deposition (CVD), epitaxial growth on silicon carbide (SiC), obtained from reduced graphene oxide (rGO) or mechanically exfoliated from graphite [3]. The measurements are made in an air filled standard R100 rectangular waveguide configuration, at one of the resonant frequency modes, typically at 7 GHz [4].

Surface conductance measurement by resonant cavity involves monitoring the resonant frequency shift and change in the quality factor before and after insertion of the specimen into the cavity in a quantitative correlation with the specimen surface area. This measurement does not explicitly depend on the thickness of the nano-carbon layer. The thickness of the specimen does not need to be known, but it is assumed that the lateral dimension is uniform over the specimen area.

PDF Catalog

PDF Pages PDF Title
4 CONTENTS
5 FOREWORD
7 INTRODUCTION
8 1 Scope
2 Normative references
3 Terms and definitions
3.1 Graphene layers
10 3.2 Measurement terminology
11 4 Microwave cavity test fixture
12 5 Test specimen
6 Measurement procedure
6.1 Apparatus
Figures
Figure 1 – Microwave cavity test fixture
13 6.2 Calibration
6.3 Measurements
6.3.1 General
6.3.2 Empty cavity
6.3.3 Specimen
14 6.3.4 Repeated procedure
6.3.5 Substrate
7 Calculations of surface conductance
8 Report
15 9 Accuracy consideration
16 Annex A (informative) Case study of surface conductance measurement of single-layer and few-layer graphene
A.1 General
A.2 Cavity perturbation procedure
17 A.3 Experimental procedure
A.4 Results
18 A.5 Surface conductance of single-layer graphene and few-layer graphene
Figure A.1 – S21 magnitude of the resonant peak TE103 as a function of frequency at several specimen insertions (hx)
Figure A.2 – Plots of 1/Qx − 1/Q0 as a function of the normalized specimen area (w hx).
19 A.6 Summary
20 Bibliography
BSI PD IEC/TS 62607-6-4:2016
$102.76