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BS ISO 5861:2024

BS ISO 5861:2024

$167.15

Surface chemical analysis. X-ray photoelectron spectroscopy. Method of intensity calibration for quartz-crystal monochromated Al Kα XPS instruments

Published By Publication Date Number of Pages
BSI 2024 36
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PDF Catalog

PDF Pages PDF Title
2 undefined
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviated terms
11 5 Requirements
5.1 General
5.2 X-ray photoelectron spectrometer
5.2.1 Operating requirements
5.2.2 Instrument geometry
12 5.3 Reference material
13 5.4 Frequency of intensity scale calibration
6 Data acquisition
6.1 General
6.2 Preparation
6.2.1 XPS Instrument
6.2.2 LDPE reference sample
6.2.3 X-ray source and electron flood source
14 6.2.4 Noise spectrum
6.3 LDPE intensity measurement
6.3.1 Spectra
15 6.3.2 Data preparation
17 7 Relative response
7.1 General
7.2 Calculation of relative response, T
7.2.1 Relative throughput inspection
7.2.2 Extension of throughput data
19 7.2.3 Relative response determination
20 7.2.4 Error in relative response
21 7.3 Use of relative response, T
7.3.1 Correction of survey spectra
7.3.2 Use in quantification
22 Annex A (informative) Flow charts
25 Annex B (normative) Table of reference kinetic energies and intensities for LDPE
27 Annex C (informative) A fitting curve for relative response
28 Annex D (informative) Examples
35 Bibliography

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BS ISO 5861:2024
$167.15